A method is described for obtaining monodomain PbTiO{sub 3} single crystals with high electrical resistivity (10{sup 10}{Omega} cm) and low dielectric frequency dispersion. The single crystals of PbTiO{sub 3} were grown by flux solution method. Space charge related defects, which result in the large dielectric frequency dispersion, were eliminated by heat treatments. 90{degrees} domains were removed by applying a unidirectional compressive stress along the <100> crystallographic direction. The monodomain single crystals of PbTiO{sub 3} were identified by cross polarized light optical microscopy and by X-ray diffraction (rocking curve). The anisotropic dielectric constants of these high quality single crystals were measured …
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A method is described for obtaining monodomain PbTiO{sub 3} single crystals with high electrical resistivity (10{sup 10}{Omega} cm) and low dielectric frequency dispersion. The single crystals of PbTiO{sub 3} were grown by flux solution method. Space charge related defects, which result in the large dielectric frequency dispersion, were eliminated by heat treatments. 90{degrees} domains were removed by applying a unidirectional compressive stress along the <100> crystallographic direction. The monodomain single crystals of PbTiO{sub 3} were identified by cross polarized light optical microscopy and by X-ray diffraction (rocking curve). The anisotropic dielectric constants of these high quality single crystals were measured as a function of temperature. The results differ from the data reported previously in the literature.
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Li, Z.; Xu, X. Z.; Dai, X. H.; Lam, D. J. & Chan, S. K.Growth, preparation, and dielectric properties of monodomain single crystal PbTiO sub 3,
article,
May 1, 1992;
Illinois.
(https://digital.library.unt.edu/ark:/67531/metadc1057120/:
accessed June 8, 2024),
University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu;
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