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The Effect of Radiation on the Corrosion of Metals by Water

Description: Technical report. Long-time tests have been made on the effect of various types of radiation on the corrosion of 2S aluminum in simulated W water. In no case was any acceleration of corrosion by the radiation observed; the effect of radiation, if any, appeared to be a protective one. Deuteron irradiation did accelerate the corrosion of mild steel at low flow rates in hot water of pH 6 to 7, but no appreciable effect was observed with copper, stainless steel, or tuballoy. The general theory … more
Date: July 6, 1944
Creator: Allen, A. O. (Augustine O.); Bowman, M. C.; Goldowski, Nathalie; Larson, R. G. & Treiman, L.
Item Type: Refine your search to only Report
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The Effects of Neutron Bombardment on the Electrical Resistance of Aluminum, Beryllium and Tuballoy (Uranium)

Description: Abstract. Wigner effects on aluminum, beryllium, and tuballoy have been studied by the electrical resistance method. Samples were exposed during an interval which would have produced an increase of approximately 22% in resistance of AGOT-K graphite. The resistance of tuballoy increased approximately 1%. It is shown that the increase can be accounted for by the amount of fission product impurity formed during the exposure. Neither aluminum nor beryllium showed any change. In the case of Be,… more
Date: November 2, 1944
Creator: Royal, J.
Item Type: Refine your search to only Report
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Electrolytic Production of Uranium from Solutions of its Tribromide in Fused Salts

Description: Abstract. the electrodeposition of uranium metal, in the form of tree-like deposits, from molten strontium halide baths is described. Under the best conditions studied, approximately 40% recovery is attained. Freedom from side-reactions of the reduced uranium with anode products and/or refractory materials, and high cathode current densities appear to be essential to the success of the process. the refining of uranium under similar conditions appears to occur quite readily, with approximatel… more
Date: August 15, 1944
Creator: Webster, Richard A.
Item Type: Refine your search to only Report
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The Extraction Method of Purification of Uranyl Nitrate

Description: Technical report. Three extractions of a diethyl ether solution of uranyl nitrate with small portions of water are effective in removing rare earths, as is shown by radio-gadolinium and radio-europium tracer experiments. A study of representative ethers, alcohols, ketones, and esters showed that diethyl ether and a mixture of 85% ethyl methyl ketone with 15% xylene are the best solvents for the extraction.
Date: August 28, 1942
Creator: Myers, L. S., Jr.; Anderson, K. C.; Wexler, Sol & Boyd, G. E.
Item Type: Refine your search to only Report
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The Extraction of Uranium into Hexone as Uranyl Thiocyanate from Thorium Nitrate Solutions

Description: Technical report with six sections describing the process: (1) The reaction of HN)3 with HSCN; (2) The distribution of nitric acid between hexone and water; (3) The distribution of HSCN between hexone and water; (4) The solubility of thorium sulfate in various extraction solutions; (5) The distribution of protoactinium and fission elements between hexone and aqueous thiocyanate solutions; and (6) Separation of uranium from thorium by extraction into hexone as UO2(SCH)a.
Date: May 18, 1945
Creator: Reas, William H.
Item Type: Refine your search to only Report
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Extraction of Uranyl Nitrate and Thorium Nitrate by Organic Solvents

Description: Abstract. The separation of uranyl nitrate from aqueous solutions of 0.635 M thorium nitrate, 3 M nitric acid and 3 M calcium nitrate by extraction with organic solvents has been investigated. Solvents which gave good separations were 2-tthyl hexyl acetate, ethyl benzoate, n-butyl either and beta-beta- dichloroethyl ether. In general, higher esters, ethers and alcohols are better for separating uranium from thorium that the lower homologues. Several solvents were tested at lower nitric acid… more
Date: November 5, 1945
Creator: Johnson, O. & Newton, A. S.
Item Type: Refine your search to only Report
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Fractionation of Fission Products and Heavy Elements by Volatilization Methods

Description: Technical report describing the attempt to separate the long lived fission product oxides by volatilization methods. A fractionization crucible was used. The fractionations give a fair idea of the relative volatilities of the longer lived fission products and also of the degrees of separation of the plutonium oxide or oxides from the fission products.
Date: August 27, 1946
Creator: Erway, N. D. & Simpson, O. C.
Item Type: Refine your search to only Report
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Healing of Fast-Neutron-Induced Changes in Graphite. II. The Effect of Heating During Exposure, Interim Report on Problem 323 MLC 2301

Description: Technical report. The effect of temperature during pile exposure on the fast-neutron-induced change in properties of graphite was studied. Temperatures up to 125 degrees C have no effect upon the rate of increase of elastic modulus; pieces exposed at 300 degrees C on the other hand show no change at all in elastic modulus. The increase in electrical resistance s an inverse function of the temperature of exposure at all temperatures in the range 60 to 300 degrees C.
Date: July 10, 1944
Creator: Neubert, Thomas A.; Novick, A.; Schenck, R. & Shapiro, E.
Item Type: Refine your search to only Report
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Healing of Fast-Neutron-Induced Changes in Graphite. III. Further Experiments on Effect of Heating During Exposure

Description: Abstract. It has been established that heating samples of graphite during exposure in a pile decreases substantially the observed changes in the elastic modulus and electrical resistance caused by the irradiation. The functional relationship between the percentage changes observed and the temperature of exposure resembles the relationship between the final percentage changes and the temperature of heat treatment after exposure (cf. report CC-1668). Anomalous results reported previously for hi… more
Date: March 3, 1945
Creator: Neubert, T. J.; Novick, A.; Schenek, R. T.; Shapiro, E. & Van Dyken, A. R.
Item Type: Refine your search to only Report
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Melting Point -- Composition Diagrams in the U-UBr3 System

Description: Abstract. A portion of the liquid-solid phase equilibrium region of the system U-UBr3 has been investigated by the method of thermal analysis. Uranium tribromide was prepared by introducing bromine vapor into a bulb containing finely divided uranium formed from the hydride. Cooling curves were obtained with tribromide and then with various compositions of tribromide and uranium. the information obtained showed that no solid sub halide exists but that the metal was soluble in the halide.
Date: December 20, 1944
Creator: Thurmond, Carl
Item Type: Refine your search to only Report
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Metallurgical Laboratory, Chemical Research - Heavy Water, Report for the Month Ending May 1, 1944

Description: Technical report with short reports on (1) Heavy water analysis and standardization, and Specific gravity of pure D2O; (2) Homogenous exponential experiment; (3) Recombination of pile gases; (4) Slurry pumping studies; and (5) Electron microscope laboratory.
Date: May 16, 1944
Creator: Hogness, T. R. (Thorfin Rusten), 1894-; Hiskey, C. F. & Eidinoff, Maxwell Leigh, 1915-
Item Type: Refine your search to only Report
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Metallurgical Laboratory, Chemical Research - Radiation Chemistry, Report for the Month Ending June 30, 1944

Description: Technical report with short reports on (1) P-9 recovery from UO2F2 solution; (2) Correlation of theories on action of radiation on matter; (3) Literature surveys on organic compounds and on chemistry of UO2F2; (4) effect of radiation on organic compounds; and (5) Effect of radiation on 100 area construction materials.
Date: July 14, 1944
Creator: Hogness, T. R. (Thorfin Rusten), 1894- & Burton, Milton, 1902-
Item Type: Refine your search to only Report
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Metallurgical Laboratory, Chemical Research - Radiation Chemistry, Report for the Month Ending May 15, 1943

Description: Technical report that information has bee obtained on the effect of beta and gamma radiation on the electrical resistance of insulating materials The results are summarized. The recovery to original resistance values has been measured. In general, the initial rate is rapid for the first few hours; the rate then decreases sharply. Certain samples show evidence of complete recovery. Effects on mechanical properties of several plastics has also been studied. Data on gas evolution from severa… more
Date: May 15, 1943
Creator: Franck, J.
Item Type: Refine your search to only Report
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Metallurgical Laboratory, Chemical Research - Radiation Chemistry, Report for the Month Ending October 31, 1944

Description: Technical report with short reports on (1) Effect of radiation on organic compounds; (2) Effect of radiation on separation processes; (3) Effect of radiation on water and aqueous systems; and (4) Effect of neutrons on graphite.
Date: November 14, 1944
Creator: Hogness, T. R. (Thorfin Rusten), 1894- & Burton, Milton, 1902-
Item Type: Refine your search to only Report
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Metallurgical Laboratory, Chemical Research - Radiation Chemistry, Report for the Period Ending January 15, 1945

Description: Technical report with short reports covering (1) Effect of radiation on water and aqueous systems; (2) Effect of neutrons on graphite; (3) Effect of radiation on solid compounds; and (4) Scattering, stopping-power, ion-pair production, etc.
Date: February 1, 1945
Creator: Burton, Milton, 1902- & Allen, A. O. (Augustine O.)
Item Type: Refine your search to only Report
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Metallurgical Laboratory, Chemical Research - Radiation Chemistry, the Effect of Radiation on Water and Aqueous Solutions of Inorganic Substances

Description: Technical report summarizing our knowledge of the chemical effects of ionizing radiation upon water and upon aqueous solutions of inorganic compounds. The types of radiation considered are beta rays, gamma and X rays, and heavy particles, notably neutrons, deuterons, alpha rays and fission recoils.
Date: February 22, 1944
Creator: Allen, A. O.
Item Type: Refine your search to only Report
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The Precipitation of Lanthanum from Solution in the Presence of Radiation

Description: Abstract. In order to anticipate radiation - chemical effects in solutions of active lanthanum, various solutions and suspensions containing lanthanum were irradiated with an electron beam. Separation of lanthanum from barium by the alcoholic HCl method is not rendered less efficient by radiation, although considerable gas evolution occurs. Suspensions of lanthanum as hydroxide and as ferrocyanide are not appreciably solubilized by radiation. Lanthanum oxalate is decomposed by radiation, is p… more
Date: April 6, 1945
Creator: Penneman, R. A. (Robert Allen), 1919-; Ghormley, J. A.; Gordon, S.; Leaf, B. & Allen, A. O. (Augustine O.)
Item Type: Refine your search to only Report
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Precipitation of Thorium Oxalate from Nitric Acid Solutions

Description: Introduction. It has been known for a long time that thorium is precipitated by oxalic acid in acid solutions, but a survey of the literature showed no study of the limits of the acidity and oxalic acid excess which yield quantitative results. V. I. Spitzin reports on the solubility of thorium oxalate in varying concentrations of several acids, but the effect of an excess oxalic acid is not included. Since solutions are sometimes presented for analysis that contain more than the recommended … more
Date: October 5, 1945
Creator: Ayers, A. S.
Item Type: Refine your search to only Report
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Preliminary Report on a Colorimetric Method for the Determination of Microgram Quantities of Thorium : Experiments in the Dissolution of O2 Metal [UO2]

Description: Abstract. thorium can be precipitated as a salt of p-dimethylaminoazophenylarsonic acid at a pH of about 1.5. the precipitate, collected on a sintered glass filter is washed with dilute ammonium hydroxide to dissolve the dye. the amount of thorium is determined by measuring the concentration of the dye spectrophotometrically at a wavelength of 450 millimicrons. Zirconium, which interferes, can be separated and determined using the same reagent in strong hydrochloric. the behavior of thorium… more
Date: January 1, 1945
Creator: Byerly, W.; Niedrach, L.; Davin, W.; Dyas, H. & Bane, R. W.
Item Type: Refine your search to only Report
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