The Use Of Scanning Probe Microscopy To Investigate Crystal-Fluid Interfaces

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Over the past decade there has been a natural drive to extend the investigation of dynamic surfaces in fluid environments to higher resolution characterization tools. Various aspects of solution crystal growth have been directly visualized for the first time. These include island nucleation and growth using transmission electron microscopy and scanning tunneling microscopy; elemental step motion using scanning probe microscopy; and the time evolution of interfacial atomic structure using various diffraction techniques. In this lecture we will discuss the use of one such in situ method, scanning probe microscopy, as a means of measuring surface dynamics during crystal growth and … continued below

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Orme, C. A. & Giocondi, J. L. April 16, 2007.

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Over the past decade there has been a natural drive to extend the investigation of dynamic surfaces in fluid environments to higher resolution characterization tools. Various aspects of solution crystal growth have been directly visualized for the first time. These include island nucleation and growth using transmission electron microscopy and scanning tunneling microscopy; elemental step motion using scanning probe microscopy; and the time evolution of interfacial atomic structure using various diffraction techniques. In this lecture we will discuss the use of one such in situ method, scanning probe microscopy, as a means of measuring surface dynamics during crystal growth and dissolution. We will cover both practical aspects of imaging such as environmental control, fluid flow, and electrochemical manipulation, as well as the types of physical measurements that can be made. Measurements such as step motion, critical lengths, nucleation density, and step fluctuations, will be put in context of the information they provide about mechanistic processes at surfaces using examples from metal and mineral crystal growth.

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PDF-file: 22 pages; size: 3.7 Mbytes

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  • Perspectives on Inorganic, Organic, and Biological Crystal Growth: from Fundamentals to Applications , The Use Of Scanning Probe Microscopy To Investigate Crystal-Fluid Interfaces, American Institute of Physics, Melville, NY 2007, pp. 342-362

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  • Report No.: UCRL-BOOK-230189
  • Grant Number: W-7405-ENG-48
  • Office of Scientific & Technical Information Report Number: 941395
  • Archival Resource Key: ark:/67531/metadc899736

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  • April 16, 2007

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  • Sept. 27, 2016, 1:39 a.m.

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  • Oct. 7, 2016, 6:07 p.m.

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Orme, C. A. & Giocondi, J. L. The Use Of Scanning Probe Microscopy To Investigate Crystal-Fluid Interfaces, book, April 16, 2007; Livermore, California. (https://digital.library.unt.edu/ark:/67531/metadc899736/: accessed June 7, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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