Chemical Properties of Sodium Triethylhydroborate and Sodium Triisopropoxyhydroborate

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Technical report abstract: Sodium hydride and triethylborane react to form sodium triethylhydroborate, NaBH(C2H5)3. This compound, a liquid at rooom temperature, was found to be soluble in hexane and mineral oil. A study was made of the thermal decomposition of sodium triethylhydroborate and its behavior toward boron trifluoride, boron trichloride, methyl borate, carbon dioxide, silane, and ethylene. Sodium triisopropoxyhydroborate, NaBH(OC3H7)3, was prepared and also found to be soluble in hexane and mineral oil. The reactions of this compound with methyl borate, triethylborane, silicon tetrachloride, and boron trichloride were investigated.

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10 pages

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Pearson, Richard King, 1926-; Edwards, L. J. & Maginnity, P. M. December 13, 1956.

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Technical report abstract: Sodium hydride and triethylborane react to form sodium triethylhydroborate, NaBH(C2H5)3. This compound, a liquid at rooom temperature, was found to be soluble in hexane and mineral oil. A study was made of the thermal decomposition of sodium triethylhydroborate and its behavior toward boron trifluoride, boron trichloride, methyl borate, carbon dioxide, silane, and ethylene. Sodium triisopropoxyhydroborate, NaBH(OC3H7)3, was prepared and also found to be soluble in hexane and mineral oil. The reactions of this compound with methyl borate, triethylborane, silicon tetrachloride, and boron trichloride were investigated.

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10 pages

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Digitized from microopaque cards (1).

Includes bibliographic references (page 10).

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  • SuDoc Number: Y 3.At 7:22/CCC-1024-TR-213
  • Report No.: CCC-1024-TR-213
  • Accession or Local Control No: metadc1256344
  • Archival Resource Key: ark:/67531/metadc1256344

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  • December 13, 1956

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  • Aug. 10, 2021, 7:37 a.m.

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  • Nov. 17, 2021, 12:42 p.m.

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Pearson, Richard King, 1926-; Edwards, L. J. & Maginnity, P. M. Chemical Properties of Sodium Triethylhydroborate and Sodium Triisopropoxyhydroborate, report, December 13, 1956; Callery, Pennsylvania. (https://digital.library.unt.edu/ark:/67531/metadc1256344/: accessed May 27, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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