TNX Evaporator Incident January 12, 1953

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Description

From abstract: "The circumstances are described pertaining to an explosion in a TNX evaporator during the concentration of a uranyl nitrate-nitric acid solution. TBP and Amsco diluent were probably present in the evaporator charge. A laboratory program involving small-scale atmospheric and closed-vessel distillations of various mixtures of UNH, HNO3, Amsco, TBP, and water indicate that an exothermic reaction between TBP and UNH, or between TBP and HNO3, or both, was responsible for the explosion. The danger areas of temperature, TBP concentration, pressure, and heating rate are defined and recommendations are made for safe evaporator operation.

Physical Description

35 pages : illustrations.

Creation Information

Colven, T. J.; Nichols, G. M. & Siddall, T. H. May 15, 1953.

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Description

From abstract: "The circumstances are described pertaining to an explosion in a TNX evaporator during the concentration of a uranyl nitrate-nitric acid solution. TBP and Amsco diluent were probably present in the evaporator charge. A laboratory program involving small-scale atmospheric and closed-vessel distillations of various mixtures of UNH, HNO3, Amsco, TBP, and water indicate that an exothermic reaction between TBP and UNH, or between TBP and HNO3, or both, was responsible for the explosion. The danger areas of temperature, TBP concentration, pressure, and heating rate are defined and recommendations are made for safe evaporator operation.

Physical Description

35 pages : illustrations.

Notes

Digitized from microopaque cards.

"Interim Technical Report."

"May 15, 1953."

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  • Report No.: DP-25
  • Grant Number: AT(07-2)-1
  • SuDoc Number: Y 3.At 7:22/DP-25
  • Accession or Local Control No: metadc1201268
  • Archival Resource Key: ark:/67531/metadc1201268

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Technical Report Archive and Image Library

The Technical Report Archive & Image Library (TRAIL) identifies, acquires, catalogs, digitizes and provides unrestricted access to U.S. government agency technical reports. The mission of TRAIL is to ensure preservation, discoverability, and persistent open access to government technical publications regardless of form or format.

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Imaged from microcard, these technical reports describe research performed for U.S. government agencies from the 1930s to the 1960s. The reports were provided by the Technical Report Archive and Image Library (TRAIL).

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Creation Date

  • May 15, 1953

Added to The UNT Digital Library

  • Aug. 15, 2019, 10:26 p.m.

Description Last Updated

  • Dec. 12, 2019, 11:06 a.m.

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Colven, T. J.; Nichols, G. M. & Siddall, T. H. TNX Evaporator Incident January 12, 1953, report, May 15, 1953; Wilmington, Delaware. (https://digital.library.unt.edu/ark:/67531/metadc1201268/: accessed May 28, 2024), University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu; crediting UNT Libraries Government Documents Department.

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