A computer-controlled three-oven gas chromatograph having a multi-position stream-switching valve has been used first to divide a wide-boiling mixture of n-alkanes into three cuts and then to fractionate each cut using a packed column at a different temperature. After initial injection of the sample into the highest temperature column, the low boilers were switched to a low temperature oven. Then, the mid-boilers were switched to a column at an intermediate temperature. For routine repetitive analyses, the multi-oven approach offers an attractive alternative.
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A computer-controlled three-oven gas chromatograph having a multi-position stream-switching valve has been used first to divide a wide-boiling mixture of n-alkanes into three cuts and then to fractionate each cut using a packed column at a different temperature. After initial injection of the sample into the highest temperature column, the low boilers were switched to a low temperature oven. Then, the mid-boilers were switched to a column at an intermediate temperature. For routine repetitive analyses, the multi-oven approach offers an attractive alternative.
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Spencer, W. A. & Rogers, L. B.Multi-temperature gas chromatography using isothermal columns in series. Technical report,
report,
August 11, 1980;
United States.
(https://digital.library.unt.edu/ark:/67531/metadc1053263/:
accessed June 3, 2024),
University of North Texas Libraries, UNT Digital Library, https://digital.library.unt.edu;
crediting UNT Libraries Government Documents Department.