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Chemical Technology Division Unit Operations Section Monthly Progress Report, September 1961

Description: Nine samples of ThO/sub 2/ -UO/sub 2/ prepared as part of the solgel process development studies showed no consistent effects from small variations in several process parameters. The reaction of methane and copper oxide was studied. Engineering studies of the continuous dissolution of simulated U-Zr-Sn fuels in 6.5 M NH4F, 0.6-1.0 M NH/sub 4/NO/sub 3/, 0.1 M H/sub 2/O/sub 2/ were continued in modified 6-in.-dia. equipment. A total of 1642 kg of U from NaK bonded SRE Core I fuel rods wad dejacke… more
Date: April 1, 1962
Creator: Whatley, M. E.; Haas, P. A.; Horton, R. W.; Ryon, A. D.; Suddath, J. C. & Watson, C. D.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Chemical Technology Division, Unit Operations Section Monthly Progress Report, June 1961

Description: An interfacial viseometer was built for use in an interfacial phenomena study. Installation of a 6-in.-ID foam separation column system was completed. The dispersiondrying-sintering characteristics of six low-nitrate batches of thoria sol material were studied. The average effective porosity of the CuO pellets used for reactor helium purification was determined to be 0.0545 for H/ sub 2/ transport and 0.0526 for CO transport. In continuous Zirflex dissolution studies, no H/sub 2/O/sub 2/ decomp… more
Date: January 23, 1962
Creator: Whatley, M. E.; Haas, P. A.; Horton, R. W.; Ryon, A. D.; Suddath, J. C. & Watson, C. D.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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TCT hybrid preconceptual blanket design studies

Description: The conceptual design of a tokamak fusion-fission (hybrid) reactor, which produces electric power and fissile material, has been performed in a cooperative effort between Princeton's Plasma Physics Laboratory (PPPL) and Battelle's Pacific Northwest Laboratories (PNL). PPPL, who had overall project lead responsibility, designed the fusion driver system. Its core consists of a tokamak plasma maintained in the two-component torus (TCT) mode by both D and T beams and having a single null poloidal d… more
Date: January 1, 1978
Creator: Aase, D. T.; Bampton, M. C. C.; Doherty, T. J.; Leonard, B. R.; McCann, R. A.; Newman, D. F. et al.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Cause of pitting in beryllium

Description: Light microscopy, bare-film radiography, secondary ion mass spectroscopy, electron microprobe and physical testing were used to examine beryllium specimens exhibiting a stratified, pitted, pattern after chemical milling. The objective was to find the cause of this pattern. Specimens were found to have voids in excess of density specification allowances. These voids are attributed, at least in part, to the sublimation of beryllium fluoride during the vacuum hot pressing operation. The origin of … more
Date: April 16, 1982
Creator: Kershaw, R. P.
Item Type: Refine your search to only Article
Partner: UNT Libraries Government Documents Department
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Energy dependence of metallic-encapsulated thermoluminescent dosimeters. Annual report

Description: The gamma-ray energy responses of encapsulated /sup 7/LiF and CaF/sub 2/:Mn thermoluminescent dosimeters were measured and compred to calculated values. This study was performed in order to improve the accuracy of gamma-ray heating measurements made in polyenergetic gamma-ray fields such as Argonne National Laboratory's Zero Power Reactors. Equations used in the development of the TERC/III computer code and code input parameters are specified. A section on TLD precision is also included. Compar… more
Date: June 1980
Creator: Simons, G. G.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Corrosion Behavior of Reactor Materials in Fluoride Salt Mixtures

Description: Molten fluoride salts, because of their radiation stability and ability to contain both Th and U, offer important advantages as high-temperature fuel solutions for nuclear reactors and as media suitable for nuclear fuel processing. Both applications have stimulated experimental and theoretical studies of the corrosion processes by which molten salt mixtures attack potential reactor materials. Corrosion experiments with fluoride salts which were conducted in support of the Molten-Salt Reactor E … more
Date: September 19, 1962
Creator: DeVan, J. H. & Evans, R. B., III
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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CHEMICAL ENGINEERING DIVISION SUMMARY REPORT, JULY, AUGUST, SEPTEMBER, 1961

Description: Development activities are reported on pyrometallurgical processes including melt refining and those using liquid metal solvents. Development of processing facilities for EBR II is also reported. In other work, laboratory- and engineering-scale investigations on fluoride volatility processes were condueted, and conversion of UF/sub 6/ to UO/sub 2/ was studied. Investigations are also reported concerning the kinetics of metal ignition and oxidation, and metalwater reactions. In work associated w… more
Date: October 31, 1962
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Phoenix I energy extraction experiment

Description: Energy extraction experiments are reported for the Phoenix I amplifier driven by a discharge-initiated oscillator-preamplifier system operating on mixtures of either SF/sub 6/-HI or SF/sub 6/-C/sub 2/H/sub 6/ and an electron-beam-initiated intermediate amplifer (lambda-3) fueled with H/sub 2/ and F/sub 2/ mixtures. When the oscillator-preamplifier system operated with mixtures of SF/sub 6/-HI the input spectrum to the Phoenix I amplifier contained approx. 28 P-branch vibrational-rotational line… more
Date: July 1, 1980
Creator: Hoffman, J. M.; Patterson, E. L.; Tisone, G. C. & Moreno, J. B.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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RIMS diagnostics for laser desorption/laser ablation

Description: Laser desorption mass spectrometry is a useful method for interrogating materials and events at or near surfaces. Laser desorption/ablation combined with Resonance Ionization Mass Spectrometry (RIMS) provides a powerful tool to obtain information on chemical composition and speciation and, in some cases, internal and translational energy distributions. The application of this technique to the interrogation of materials and interfaces is discussed for several systems, including the analysis of c… more
Date: January 1, 1986
Creator: Apel, E. C.; Nogar, N. S.; Miller, C. M. & Estler, R. C.
Item Type: Refine your search to only Article
Partner: UNT Libraries Government Documents Department
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Sodium Fluozirconate Precipitation Process for Zirconium Fuels. Part 1. Laboratory Development

Description: Precipitation, evaporation, and extraction feed preparation conditions are established for the removal of zirconium and fluoride from fuel dissolver product solutions by the addition of sodium formate. A sparingly soluble complex fluozirconate is formed. Ninety-five to 99% of the zirconium and fluoride is separated from the uranium losses of 0.1% or less. Chemical material balances, based on experimental data, were developed for two flowsheets. In one flowsheet, sufficient nitric acid is added … more
Date: May 15, 1962
Creator: Newby, B. J.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Manual of analytical methods for the Industrial Hygiene Chemistry Laboratory

Description: This Manual is compiled from techniques used in the Industrial Hygiene Chemistry Laboratory of Sandia National Laboratories in Albuquerque, New Mexico. The procedures are similar to those used in other laboratories devoted to industrial hygiene practices. Some of the methods are standard; some, modified to suit our needs; and still others, developed at Sandia. The authors have attempted to present all methods in a simple and concise manner but in sufficient detail to make them readily usable. I… more
Date: August 1, 1991
Creator: Greulich, K. A. & Gray, C. E.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Gas breakers for tokamak OHMIC-heating duty

Description: The current interrupting capacity of air blast and SF/sub 6/ breakers is reviewed for application in tokamak ohmic-heating circuits. Particular attention is paid to generator breakers for their large current interrupting capacity and suitability for ohmic-heating circuits.
Date: January 1, 1977
Creator: Vogel, H.F.
Item Type: Refine your search to only Article
Partner: UNT Libraries Government Documents Department
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Investigation of breached depleted UF sub 6 cylinders

Description: In June 1990, during a three-site inspection of cylinders being used for long-term storage of solid depleted UF{sub 6}, two 14-ton cylinders at Portsmouth, Ohio, were discovered with holes in the barrel section of the cylinders. An investigation team was immediately formed to determine the cause of the failures and their impact on future storage procedures and to recommend corrective actions. Subsequent investigation showed that the failures most probably resulted from mechanical damage that oc… more
Date: January 1, 1991
Creator: DeVan, J. H.
Item Type: Refine your search to only Article
Partner: UNT Libraries Government Documents Department
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CHEMICAL TECHNOLOGY DIVISION ANNUAL PROGRESS REPORT FOR PERIOD ENDING MAY 31, 1961

Description: Activities in research programs are summarized in the areas of power reactor fuel processing, fluoride volatility processing, molten salt reactor fuel processing, homogeneous reactor fuel processing, waste treatment and disposal pilot plant decontamination, GCR coolant purification studies, equipment decontamination, HRP thoria blanket development, fuel cycle development, transuranium element studies, production of U/sup 232/, uranium processing, fission product recovery, thorium recovery from … more
Date: September 21, 1961
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Dielectric strengths of new gases and gas mixtures

Description: It is emphasized that the most effective gaseous dielectrics are gas mixtures with components chosen on the basis of fundamental physicochemical knowledge, especially on low-energy electron-molecule interactions. On the basis of such lnowledge, especially on electron attachment and electron slowing down, a number of new gases and gas mixtures have been found with breakdown strengths superior to pure SF/sub 6/. These include the unitary gases c-C/sub 4/F/sub 8/ (perfluorocyclobutane), C/sub 4/F/… more
Date: January 1, 1978
Creator: James, D.R.; Christophorou, L.G.; Pai, R.Y.; Pace, M.O.; Mathis, R.A.; Sauers, I. et al.
Item Type: Refine your search to only Article
Partner: UNT Libraries Government Documents Department
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Diagnosing vegetation injury caused by air pollution

Description: The structure and function of plants in relation to air pollution injury is discussed. The sources, atmospheric chemistry, monitoring data, symptomatology, factors affecting plant response, injury threshold doses, air quality standards, relative sensitivity of plants, and leaf tissue analysis are discussed for major air pollutants. Among the pollutants discussed are: the photochemical oxidants (ozone, PAN, nitrogen oxides, sulfur dioxide, and fluorides). Minor pollutants discussed in the same f… more
Date: February 1, 1978
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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MHD compressor---expander conversion system integrated with GCR inside a deployable reflector

Description: This work originates from the proposal MHD Compressor-Expander Conversion System Integrated with a GCR Inside a Deployable Reflector''. The proposal concerned an innovative concept of nuclear, closed-cycle MHD converter for power generation on space-based systems in the multi-megawatt range. The basic element of this converter is the Power Conversion Unit (PCU) consisting of a gas core reactor directly coupled to an MHD expansion channel. Integrated with the PCU, a deployable reflector provides… more
Date: April 20, 1989
Creator: Tuninetti, G. (Ansaldo S.p.A., Genoa (Italy). Research Div.); Botta, E.; Criscuolo, C.; Riscossa, P. (Ansaldo S.p.A., Genoa (Italy). Nuclear Div.); Giammanco, F. (Pisa Univ. (Italy). Dipt. di Fisica) & Rosa-Clot, M. (Florence Univ. (Italy). Dipt. di Fisica)
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Experimental investigation of the chemistry of excited states of rare gases. First quarterly progress report, October 15, 1977--January 15, 1978

Description: The quenching of XeF(B) was studied using the steady-state photolysis of XeF/sub 2/ as the source of XeF(B). The product states from the sensitized reaction of Xe(/sup 3/P/sub 1/) with Cl/sub 2/ and COCl/sub 2/ also were studied. The new XeF(B) quenching rate constants are described. The pulsed laser induced fluorescence technique was used to measure radiative lifetimes and two-body quenching rate constant (with Ar) for the low energy Xe(6p)* states. Serious signal/noise problems for the lowest… more
Date: February 1978
Creator: Setser, D. W.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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Uranium hexafluoride: Safe handling, processing, and transporting: Conference proceedings

Description: This conference seeks to provide a forum for the exchange of information and ideas of the safety aspects and technical issue related to the handling of uranium hexafluoride. By allowing operators, engineers, scientists, managers, educators, and others to meet and share experiences of mutual concern, the conference is also intended to provide the participants with a more complete knowledge of technical and operational issues. The topics for the papers in the proceedings are widely varied and inc… more
Date: January 1, 1988
Creator: Strunk, W.D. & Thornton, S.G. (eds.)
Item Type: Refine your search to only Article
Partner: UNT Libraries Government Documents Department
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Radiation standards and calibrations. FY-1981 annual report

Description: The research program encompasses: reviewing calibration standards, regulations, and handbooks; assuring that calibration procedures used are in agreement with technically accepted methods; maintaining basic radioactive sources and instruments that serve as radiological standards; and providing traceability to the National Bureau of Standards where possible. In addition, major efforts are being expended to upgrade the 318 calibration facility. This report focuses on major accomplishments during … more
Date: July 1, 1982
Creator: Roberson, P. L.; Yoder, R. C.; Fox, R. A.; Hooker, C. D.; Hogan, R. T.; Holbrook, K. L. et al.
Item Type: Refine your search to only Report
Partner: UNT Libraries Government Documents Department
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