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Final Report on Recovery of Thorium and Uranium From Monazite Sand : Volume 1

Description: Report describing a method for recovery of high yields of thorium and uranium from monazite sand concentrates. Monazite is decomposed into hydrous metal oxides, which are dissolved in an acid. The solution is then separated into a precipitate, which seperates from thorium and uranium. An alternate separation method is evaluated.
Date: September 15, 1950
Creator: Calkins, G. D.; Filbert, R. B., Jr.; Bearse, A. E. & Clegg, J. W.
Partner: UNT Libraries Government Documents Department
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Final Report on Purification of Thorium Nitrate by Solvent Extraction With Tributyl Phosphate: 1. Laboratory Investigations

Description: Report discussing laboratory investigations of thorium nitrate purification. Batch equilibrium data, solubility data, viscosity data, density data, and the results seven batch countercurrent extraction tests and two selective stripping tests are included.
Date: July 31, 1952
Creator: Ewing, R. A.; Fishel, J. B.; Kiehl, S. J., Jr.; Sharpe, R. E. & Bearse, A. E.
Partner: UNT Libraries Government Documents Department
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Zirconium Research and Development : Progress Report

Description: From introduction: "This is the ninth monthly report, BMI-514, under Contract No. AT(30-1)-771 on "Zirconium Research and Development". The report covers the work period from September 15, 1950, to October 15, 1950. Work is continuing on the preparation of large-diameter zirconium crystal bars in the 16-inch-diameter de Boer unit. Crystal bars up to 1-5/16 inches in diameter and 8 feet long have been prepared in this unit."
Date: October 15, 1950
Creator: Bulkowski, H. H.; Sebenick, J. J.; Campbell, Ivor E. & Gonser, B. W.
Partner: UNT Libraries Government Documents Department
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Grain Refinement of Uranium by Alloying

Description: Binary alloys of uranium with 38 elements in the range 0.01 to 1.0 at.% were made. Three alloys having nominal compositions of 0.01, 0.1, and 1.0 at.% were made with most of the elements, and in addition, 12 ternary and quaternary alloys were made. The alloys were cast, rolled to 7/8-inch-diameter bars, heat treated, and examined for grain size.
Date: June 1, 1951
Creator: Saller, Henry A.; Keeler, J. R. & Eddy, N. S.
Partner: UNT Libraries Government Documents Department
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Delta-Phase Zirconium Hydride as a Solid Moderator

Description: Abstract: "In a study of the preparation and properties of delta-phase zirconium hydride it was found that large, sound bodies of the hydride can be prepared by direct combination of the elements if the rate of the reaction is retarded by limiting the supply of available hydrogen. Specimens up to 1-in. diameter were prepared using this technique. Because delta phase zirconium hydride does not readily form eutectics with iron-and nickel-base alloys below 1800 F these materials may be utilized fo… more
Date: December 18, 1957
Creator: Vetrano, James B.
Partner: UNT Libraries Government Documents Department
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The Determination of Rare Earths in Thorium

Description: Abstract: "A quantitative method for the determination of individual rare earths in thorium down to a level of 0.05 ppm, is described. The procedure consists of a chromatographic cellulose-columns separation followed by a solution-type spectrographic determination. Values are given for the recovery of a number of rare earths using this combined procedure."
Date: May 15, 1952
Creator: Center, E. J.; Henry, W. M. & Householder, R. D.
Partner: UNT Libraries Government Documents Department
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The tensile strength of solid-state bonded aluminum and nickel-plated uranium

Description: A report intended to aid in the evaluation of solid-state bonding techniques for cladding natural-uranium fuel-element cores with aluminum, tensile specimens which are 1/4 in. in diameter and 3 in. long.
Date: 1954
Creator: Saller, Henry A.; Dickerson, R. F. & Carlson, R. J.
Partner: UNT Libraries Government Documents Department
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Properties of Arc-Melted Chromium-Base Alloys

Description: From abstract: "Twelve binary chromium-base alloy systems were screened for hot workability, oxidation resistance, and hot strength using small ore-melted ingots...Experiments with the preparation of large chromium-base alloy ingots showed that cold-mold ore melting was not suitable for preparing ingots containing over about 1 w/o of alloy addition."
Date: July 14, 1958
Creator: Maykuth, Daniel J.; Roberts, John W., Jr. & Jaffee, Robert Isaac, 1917-
Partner: UNT Libraries Government Documents Department
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Estimated Manufacturing Costs for the Recovery of Thorium and Uranium from Monazite Sand

Description: Abstract: "Costs have been estimated for the production of uranium and pure thorium from monasite concentrates by a process involving (1) reaction of monasite with caustic soda, (2) dissolution of the hydrous oxides in hydrochloric acid, (3) separation from the bulk of the rare earths by hydroxide precipitation of thorium and uranium, and (4) purification by solvent extraction."
Date: September 15, 1950
Creator: Calkins, G. D. & Filbert, R. B., Jr.
Partner: UNT Libraries Government Documents Department
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Identification of Slag Constituents from Uranium Metal Production Bombs

Description: Abstract: "X-ray and microscopic examination of slags from uranium metal production bombs which gave good and bad yields in the plant at St. Louis have indicated the significance of uranium oxide formation. Apparently the oxide (UO2) results from reaction of the UF4 with linear material, particularly with moisture in the liner."
Date: January 31, 1952
Creator: Vaughan, D. A.; Cocks, G. G. & Schwartz, C. M.
Partner: UNT Libraries Government Documents Department
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The Rolling of Thorium Rod

Description: Report discussing the rolling of thorium rods. Abstract: "Thorium rods, 1-7/16 inch in diameter, were rolled from Ames castings. The billets were roughed down in diamond-grooved rolls and finished in hand-rounding rolls. Remelted chips as well as primary-metal castings were rolled, and both yielded satisfactory rods. The surface quality of the rods was generally excellent, and the machined slugs were free of seams."
Date: December 19, 1951
Creator: Saller, Henry A.; Keeler, J. R. & Donley, R. J.
Partner: UNT Libraries Government Documents Department
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Mineralogical Examination of Pitchblende Concentrates and Nitric Acid Digest Residues

Description: This report has two parts to it discussing mineralogical examination of pitchblende concentrates and nitric acid digest residues. Part I gives the results of a cursory examination with the petrographic microscope of samples of pitchblende concentrates and residues to see if there is a relationship between the mineral composition of the samples and the filterability of the residue. Part II gives a revaluation of the data in Report BMI-241 on the mineral composition of two residues from the nitri… more
Date: February 9, 1951
Creator: Scott, D. W.; Tangel, O. F. & Richardson, A. C.
Partner: UNT Libraries Government Documents Department
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Identification of Reaction Products Formed During Magnesium Reduction of Uranium Tetrafluoride: Report

Description: Abstract: "This report describes the results of X-ray diffraction examination of reaction products from a series of experiments performed by Mallinckrodt Chemical Works as an acid in understanding the process of bomb reduction of UF4. UF4 is initially reduced to UF3 by magnesium at 560 C., and subsequently to metal at 600 C. MgF2 from the initial reaction forms a coating on the magnesium which retards the final spontaneous reaction."
Date: May 15, 1953
Creator: Schwartz, C. M. & Vaughan, D. A.
Partner: UNT Libraries Government Documents Department
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Zirconium Pilot Plant Research and Development Progress Report

Description: The following report studies the effect of flow rates and deposition pressure on the zirconium deposition in the zirconium pilot plant with the use of a Hilco oil purifier for the vacuum pumps that permitted studies to continue through the month.
Date: November 20, 1951
Creator: Dryden, C. E.; Accountius, O. E.; Black, D. G.; Finney, B. C.; Gruber, B. A.; Jurevic, W. G. et al.
Partner: UNT Libraries Government Documents Department
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Zirconium Pilot Plant Research and Development Progress Report

Description: The following progress report was compiled by the research and development division of the zirconium pilot plant. This report discusses two iodination and deposition runs that were completed as of August 20, 1951, as well as the third iodination run that uses a vaporizer condenser that condenses approximately 40 pounds of zirconium iodide.
Date: September 20, 1951
Creator: Accountius, O. E.; Black, D. G.; Dryden, C. E.; Finney, B. C.; Gruber, B. A.; Jurevic, W. G. et al.
Partner: UNT Libraries Government Documents Department
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Electrodeposition of Aluminum on Uranium

Description: Abstract: "Aluminum electroplating was studied in a search for new methods of cladding uranium fuel elements. Uranium electroclad with 12 mils of aluminum over a 0.5-mil (or nickel plus copper) electroplate resisted corrosion for more than 100 hr in boiling water. This quality of protection was effected by hot pressing the electroclad uranium with 5.1 tons per sq in. for 5 min at 950 F. The electroclad uranium with hot-pressed samples paralleled those of later experiments with hot-pressed wroug… more
Date: March 30, 1955
Creator: Beach, John G.; Schickner, William C.; Hopkinson, Dolores. & Faust, Charles L.
Partner: UNT Libraries Government Documents Department
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Determination of Rare Earths in Refined Uranium : Topical Report

Description: Abstract: "Rare-earth analyses were performed on several samples of refined uranium oxide and nitrate, using a modified cellulose column procedure. Rare earths were not detectable in samples of 0.03 shotgun of less. Detection limits were from 0.0005 to 0.015 ppm. Negligible quantities of low-cross-section rare earths were found in less pure uranium samples, obtained during start-up operations of the pilot plant at the Feed Materials Production Center, primarily those rare earths of greater than… more
Date: June 30, 1953
Creator: Ewing, R. A. & Bearse, A. E.
Partner: UNT Libraries Government Documents Department
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Evaluation and Consolidation of Electrolytic Thorium

Description: Abstract: "Sound, fabricable ingots of thorium were produced by triple are melting of electrolytic thorium. Consumable electrodes were fabricated by tack welding of cold-pressed and vacuum-sintered bars of the granular thorium electrodeposited from a molten-salt bath. The hydrogen content of the electrodeposited material was reduced from 80 to 4 ppm by vacuum sintering at 1250 C at pressures below 1 x 10-(-3) mm of mercury. Both sodium and chlorine content were reduced during melting; sodium fr… more
Date: June 15, 1955
Creator: Saller, Henry A.; Dickerson, Ronald F. & Foster, Ellis L.
Partner: UNT Libraries Government Documents Department
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Bonding of uranium and zirconium alloys

Description: Report describing a study of fabricating conditions for bonding zirconium and uranium alloys by roll cladding.
Date: 1953
Creator: McIntire, H. O.; Hucek, H. J. & Manning, G. K.
Partner: UNT Libraries Government Documents Department
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Reaction of Hydrogen With Uranium

Description: Report discussing reaction of hydrogen with uranium in a range of temperatures and pressures. Experimental materials, methods and results are included.
Date: February 17, 1955
Creator: Albrecht, William M. & Mallett, Manley William, 1909-
Partner: UNT Libraries Government Documents Department
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The Roll Cladding of Uranium With Aluminum

Description: Report discussing a study regarding rolling as a technique for making uranium fuel elements that are flat-plate and aluminum-clad.
Date: August 3, 1954
Creator: Saller, Henry A.; Paprocki, Stan J. & Delaney, J. F.
Partner: UNT Libraries Government Documents Department
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Progress Report on the Concentration of Pitchblende

Description: Abstract: "Additional work on the flotation of sulphides from high-sulphur pitchblende is described. Data needed for the selection of flotation equipment are presented."
Date: June 30, 1950
Creator: Wesner, A. L.; Tangel, O. F. & Richardson, A. C.
Partner: UNT Libraries Government Documents Department
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Ternaries of the eutectic uranium-chromium alloy

Description: A report about a study about the effect of small additions of iron, nickel, and manganese to the uranium - 5 wt % chromium eutectic alloy.
Date: 1953
Creator: Saller, Henry A.; Rough, Frank A. & Bauer, A. A.
Partner: UNT Libraries Government Documents Department
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