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open access

Synthesis of heterocycles: Indolo (2,1-a) isoquinolines, renewables, and aptamer ligands for cellular imaging

Description: In this thesis, we explore both total syntheses and methodologies of several aromatic heterocyclic molecules. Extensions of the Kraus indole synthesis toward 2-substituted and 2,3-disubstituted indoles, as well as biologically attractive indolo[2,1-a]isoquinolines are described. Recent renewable efforts directed to commodity maleic acid and the first reported furan-based ionic liquids are described. Our total synthesis of mRNA aptamer ligand PDC-Gly, and its dye coupled forms, plus aminoglycosi… more
Date: May 7, 2013
Creator: Beasley, Jonathan
Partner: UNT Libraries Government Documents Department
open access

Templated synthesis of nickel nanoparticles: Toward heterostructured nanocomposites for efficient hydrogen storage

Description: The world is currently facing an energy and environmental crisis for which new technologies are needed. Development of cost-competitive materials for catalysis and hydrogen storage on-board motor vehicles is crucial to lead subsequent generations into a more sustainable and energy independent future. This thesis presents work toward the scalable synthesis of bimetallic heterostructures that can enable hydrogen to compete with carbonaceous fuels by meeting the necessary gravimetric and volumetri… more
Date: May 7, 2013
Creator: Nelson, Nicholas Cole
Partner: UNT Libraries Government Documents Department
open access

Measurement of branching fractions of B decays to K1(1270)pi and K1(1400)pi and determination of the CKM angle alpha from B0 --> a1(1260) - pi-

Description: In the Standard Model, CP violation in weak interactions involving quarks is parameterized by an irreducible complex phase in the Cabibbo-Kobayashi-Maskawa (CKM) quark-mixing-matrix. The precise determination of the CKM elements is a necessary ingredient for a stringent test of the Standard Model predictions, and is a crucial input for reducing the theoretical error in many New Physics searches with flavor, e.g., in the kaon sector. The unitarity of the CKM matrix is typically expressed as a tr… more
Date: February 7, 2011
Creator: Stracka, Simone & /SLAC, /Milan U.
Partner: UNT Libraries Government Documents Department
open access

Measurement and Modeling of Blocking Contacts for Cadmium Telluride Gamma Ray Detectors

Description: Gamma ray detectors are important in national security applications, medicine, and astronomy. Semiconductor materials with high density and atomic number, such as Cadmium Telluride (CdTe), offer a small device footprint, but their performance is limited by noise at room temperature; however, improved device design can decrease detector noise by reducing leakage current. This thesis characterizes and models two unique Schottky devices: one with an argon ion sputter etch before Schottky contact d… more
Date: January 7, 2010
Creator: Beck, P R
Partner: UNT Libraries Government Documents Department
open access

Solid state NMR method development and studies of biological and biomimetic nanocomposites

Description: This thesis describes application and development of advanced solid-state nuclear magnetic resonance techniques for complex materials, in particular organic-inorganic nanocomposites and thermoelectric tellurides. The apatite-collagen interface, essential for understanding the biomineralization process in bone and engineering the interface for controlled bio-mimetic synthesis and optimized mechanical properties, is buried within the nanocomposite of bone. We used multinuclear solid-state NMR to … more
Date: February 7, 2011
Creator: Hu, Yanyan
Partner: UNT Libraries Government Documents Department
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