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The Alkaline Method for Treatment of High Radiation Level Aluminum Wastes

Description: The method is based on caustic precipitation and centrifugation (which removes the Cs and small amounts of Sr, rare earths, Zr, Nb, and Ru). These are removed in the supernatant and run through a cation exchange column. This separates Zr-NB and Ru. The effluent is precipitated and the Zr-Nb is stored in an asphalt pit. The Ru then may be recovered from the precipitate. The precipitate from the original centrifugation is calcined, pressed and transported to a deep well.
Date: January 17, 1957
Creator: Higgins, I. R.
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APPR-1 Type Absorber Rod Irradiation Test -- Irradiation Request ORNL MTR-29

Description: In order to evaluate the behavior of an APPR type absorber rod, an irradiation test program has been established. Approximately 21 more samples are planned for testing under this request. The request proposes testing a full size APPR-1 type control rod in the MTR. The objective of the test is to better evaluate the neutron absorbing material proposed for the APPR-1 control rod.
Date: January 4, 1957
Creator: Gross, E. E. & Schaffter, L. D.
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Calculation of Shield Induced Gamma Radiation Escaping Through Openings in a Biological Shield -- Application to the HRT

Description: A method was developed for calculating shield induced gamma radiation escaping through openings in a biological shield. The method was applied to the HRT and the results indicated that the contribution to the dose from induced activity in the HRT shield was around 0.1 r/hr and was insignificant in comparison to to other mechanisms contributing to the escape of gamma rays through shield openings.
Date: January 11, 1957
Creator: Claiborne, H. C. & Fowler, T. B.
open access

Carbon Steel in High Temperature Water

Description: Resistance of carbon steel to corrosion in oxygenated high-temperature (250C) water was unexpectedly good at high oxygen concentration. Pertinent literature, critically examined, and toroid experiments indicted that at low oxygen concentration attack did increase with concentration, but as oxygen concentration was sufficiently increased, more protective films were formed on the metal. Some corrosion factors in the application of carbon steel to nuclear reactors systems are discussed.
Date: January 31, 1957
Creator: Moore, G. E.
open access

Catalysts for Recombination of Radiolytic Gases Over Thorium Oxide Slurries

Description: Catalysts for use in recombining the gases produced by the radiolytic decomposition of water in thorium oxide slurries under neutron irradiation were investigated in out-of-pile tests using stoichiometric mixtures of hydrogen and oxygen. Most favorable results were obtained with a molybdenum oxide catalyst. Satisfactory rate also were attained with palladium and silver oxides. Copper, nickel, vanadium and chromium compounds were less effective.
Date: January 29, 1957
Creator: Morse, L. E.
open access

The Chemical Processing of Two-Region Aqueous Homogenous Reactors

Description: A promising scheme for the chemical processing of a thorium breeder reactor of the two-region aqueous homogeneous type consists of the following operations: concentration of insoluble fission and corrosion products from the core system into a small volume of fuel solution, combining this slurry with irradiated thorium oxide slurry taken from the blanket, recovery of D2O by evaporation, dissolution of the thorium and uranium in HNO3, and, after a suitable cooling period, recovery of the uranium … more
Date: January 29, 1957
Creator: Ferguson, D. E.
open access

Cracks in HRT Flange Bolts and Ferrules

Description: When it was discovered that two HRT flange bolts of a lot of 16 spares contained serious cracks, a program was launched to (1) determine the cause for the cracking, and (2) find methods for non-destructive testing the remainder of the 672 bolts shipment, a large portion of which had been installed in the HRT. Concurrently, inspection of 8 ferrules removed from an HRT flange revealed hairline cracking in 4 of them. Magnaglo, a magnetic particle inspection method using a fluorescent dye, proved t… more
Date: January 29, 1957
Creator: Hammond, J. P.; Adamson, G. M. & Kegler, T. M., Jr.
open access

Cross Section Program at ORNL

Description: Short reports to the members of the Nuclear Cross Section Advisory Group from three groups: (1) High voltage group; (2) Fast chopper time-of flight spectrometer; and (3) Electronuclear research division.
Date: January 21, 1957
Creator: Harvey, J. A. & Fowler, J. L. (Joseph L.)
open access

Delay Time Prior to Dumping the HRT

Description: Some refined calculations have been made, relative to a proposed delay prior to a dump, to determine the expected D2 concentration in the vent stream from the pressurizer gas bleeds during a dump of the Homogeneous Reactor Test (HRT). These calculations indicate that for vent valves have a Cv of 0.07 (venting time from 2000 psia to D2O saturation pressure of approximately 12 minutes), a delay period is not required since the D2 concentration is well below lower explosive limit. For vent valves … more
Date: January 10, 1957
Creator: Gift, E. H. & McLain, Howard A.
open access

Determination of Submicron Particle Sized by an Activation Analysis - Centrifugation Method

Description: The feasibility of determining particle sizes in the submicron range by employing an activation analysis - centrifugation method has been demonstrated. It is believed that this method is now applicable to the analysis of thorium oxide for submicron particles. The same techniques are, in most instance, usable in determining particle sized in other sample materials.
Date: January 29, 1957
Creator: Bate, L. C. & Leddicotte, G. W.
open access

Eddy-Current Measurement of Clad Thickness on Mark X MTR Fuel Plates

Description: At the request of the Alloy Preparation Group, the Nondestructive Test Development Group investigated the feasibility of determining the clad thickness on Mark X MTR Fuel Plates. As the use of induced eddy-currents was considered to be the most promising approach, a prototype instrument and probe coil utilizing this principle was developed to measure clad thickness. The results of the investigation conducted with this instrument indicate that the clad thickness of this type of fuel plats can be… more
Date: January 23, 1957
Creator: Oliver, R. B.; Allen, J. W. & Nance, Roy A.
open access

Estimated Gamma Radiation Levels at Access Holes in the HRT Shielding

Description: An estimate has been made of the gamma radiation levels at access holes in the HRT Shielding when the plugs have been removed to service or maintain the reactor. In every case the radiation level at the holes was greater than the maximum permissible exposure rate of 0.3 roentgens per week. The radiation through the holes can be attenuated to some extent by flooding the reactor cell up to the flange to be disconnected. However, shielding would still be required and it is more practical to provid… more
Date: January 24, 1957
Creator: Collins, C. W.
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Estimation of the Thermal Conductivity and the Viscosity of Gases at High Pressure

Description: Few data exist for the thermal conductivity and viscosity of gases at very high pressure. The possibility of using gases for heat transfer media at pressures up to 100 atmospheres and above raised the problem of estimating variations in the conductivity and viscosity at high pressure. Generalized plots are presented which are based on the work of Enskog, Eucken, and Hirschfelder et al. Some pertinent data from Hirschfelder et al and from Hilsenrath et al are presented.
Date: January 17, 1957
Creator: Lyon, Richard Norton
open access

Examination of 6" Diameter "O" Ring from HRT Mockup. Metallography Report (Y-12) No. 39

Description: A six-inch diameter "O" ring from the HRT Mockup was examined metallographically after 2452 hours exposure to uranyl sulfate solution at 300C. surface defects, except for cold work defects were found only in areas exposed to uranyl sulfates. Defects found were pits, transgranular cracks, surface cracks, and grain attacks.
Date: January 15, 1957
Creator: Kegley, T. M., Jr.
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Extraction of the elements with Tris-2-Ethylhexyl- and Trihexylphosphine oxides from Acidic Solutions

Description: This technical report is the second of a series which concerns the separation of ions by solvent extraction with trialkyl phosphine oxides (TOPO). This investigation has consisted in the extraction of various ions from acidic solutions with extractants that are representative of these ore specific phosphine oxides - triphenylphosphine oxide (THPO) and tris-2-ethylhexylphosihine oxides (TEHPO). In general it is observed that: (a) the order of increasing capacity of extraction is THPO > TOPO >TEH… more
Date: January 2, 1957
Creator: Ross, W. J. & White, J. C.
open access

High Pressure Flange Studies

Description: Twenty-five hundred psi ring-type flanges, ring gaskets, bolts, and special connectors were tested for adaptability to the aqueous homogenous reactor. High pressure line closures were studied to obtain empirical data pertinent to the selection or design of a connector capable of withstanding sustained thermal cycling and high pressures encountered in the aqueous homogenous reactor. Specialized stress-strain measurement techniques yielded information concerning flange deformation, ring type gask… more
Date: January 5, 1957
Creator: Fritz, K. J.
open access

The HRT Refrigerating System

Description: The HRT refrigeration system was designed to use Freon-11 (CCI3F) as the refrigerant material in the secondary loop. A Van de Graaff irradiation of this material indicated that serious corrosion problems were probable if Freon were used in the proposed metal system. A survey was made of candidate refrigerants, and Amsco 125-82 and triethyl phosphate were selected for irradiation and physical-property determinations.
Date: January 9, 1957
Creator: Silverman, M. D.
open access

HRT Sampler Development

Description: A prototype sampler for obtaining samples of high radioactive UO2SO4 solution for use in the HRT is presented. It was successfully operated in conjunction with a low pressure water system and a high pressure, high temperature UO2SO4 system.
Date: January 22, 1957
Creator: Hannaford, B. A.
open access

HRT Source Shield Calculations

Description: Calculations indicate that the proposed shielding arrangement will give a dose rate at the surface of the water tank of about 100 mrem per hr., practically all gammas. This is adequate for transportation and handling, but if the radiation actually proves to be this high, a storage location isolated from normal working areas must be provided. The isolation area need not be large, however, since the calculated dose rate at 10 feet from the shielded sources is only 3.5 mrem pr hr. For the short ti… more
Date: January 8, 1957
Creator: Haubenreich, P. N. & Rivenbark, G. W.
open access

HRT Temperature Measurement System - Issue No. 3

Description: The following temperature measurement tabulation consists of two parts. Part I lists all HRT thermocouples, their location, the junction box thru which the leads pass, and their termination, if on an instrument. Part II lists all temperature read out instruments and their location. A total of 577 thermocouples are listed in this tabulation. The roughly 77,000 ft of wire used in connecting them up cost $6,799. Temperatures are read on 24 instruments. Cost of these was approximately $15,688. Acce… more
Date: January 17, 1957
Creator: Grimes, J. D.
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Metallurgical Examination of HRT Leak Detector Tubing and Flanges

Description: After several failures had occurred in the HRT leak detector system, several lengths of this tubing were removed for metallurgical examination. The tubing was of type 304 stainless steel and was 1/4" in diameter with a 0.065 wall. The tubing had been purchased as three different lots, the first in 45 ft. lengths and the other two as standards lengths. Tubing from the first lot was used primarily for the shield penetration and, therefore, sections of it are present in all lines of the system. It… more
Date: January 31, 1957
Creator: Adamson, G. M; Hammond, T. M.; Kegley, T. M. & White, J. K.
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